Analytical Chemistry
Chemistry 255/256
Fall 2002

Course Calendar

Data and Statistics  |  Solubility, Acid/Base and Simultaneous Equilibria
Electrochemistry | SpectroscopyChromatography and Separations





Data and Statistics

9/5 Class 1:  Introduction to role-playing laboratories and classes.
Workshop:  Preparing a Professional Quality Graph


9/10 Class 2:  Standard deviations, confidence intervals, and Statistical Tests.


9/12 Class 3:  Statistical and round robin testing of laboratory data using the Q-test, t-test and F-test.
Workshop:  BP data

 

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Solubility, Acid/Base and Simultaneous Equilibria

9/17 Class 4:  Literature Searching using SciFinder Scholar, Web of Science and Other Tools.  Reference Management with End Note.  Solubility 1-control of solution species and composition with common ions


9/19 Class 5 Quiz 1 (20 min.)
Alpha fractions as computational tools in equilibria problems.
Workshop:  Alpha Fractions


9/24 Class 6:  Solubility 2 - Computational tools and pH control of solution composition.


9/26 Class 7:  Solubility 3 - Effect of ionic strength (activities) on solubility.
Workshop:  Ionic Strength effects
 


10/1 Class 8:  Examination 1
Covering Classes 1-7, Labs 1-3 , ProbSets 1-3, & DAIT 1-2


10/3 Class 9:  Acid/Base 1 - How to do monoprotic weak acids and buffer solutions.


10/8 Class 10
Acid/Base 2 - How to approach polyprotic buffer equilibria problems.
 


10/10 Class 11
Acid/Base 3 - Amphoteric buffer systems and pH problems.


10/15 Class 12
Acid/Base 4 - Polyprotic titrations and stoichiometry.

10/17 Class 13:  Quiz 2 (20 Min.)
Acid Base 5 - Titrations as an analytical method for assaying acids and bases.
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Spectroscopy

10/24 Class 14:  Spectrophotometry 1 - Interaction of light with matter, in particular atomic spectroscopy.


10/29 Class 15:  Spectrophotometry 2 - Spectrophotometers and UV systems.


10/31 Class 16:  Spectrophotometry 3 - Applications of Spectroscopy
Workshop:  Spectroscopy of Mixtures

11/5 Class 17:  Examination 2
Covering Classes 9-16, Labs 5-9, ProbSets 4-8, & DAIT 3-6
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Electrochemistry

11/7 Class 18:  Redox 1- Equilibrium cell potentials via the IUPAC conventions & the Nernst equation

11/12 Class 19:  Redox 2 - Applying the Nernst equation to potentiometric titrations.


11/14 Class 20:  Redox 3 - Applying the Nernst equation to potentiometric titratioins.


Chromatography and Separations

11/19 Class 21:  Quiz 3 (20 Min.)
Separations 1 - Solvent Extraction as a single stage chromatography experiment


11/21 Class 22:  Separations 2 - Theoretical plates, peak shape and gas chromatography.


11/26 Class 23:  Separations 3 - Pumps and columns in HPLC.

12/3 Class 24:  Separations 3 - Columns, and detectors in HPLC.


12/5 Class 25:  Separations 4 - Workshop: analysis of chromatogram and the quality of separation

12/10 Class 26:  Examination 3
Covering Classes 18-25, Labs 10-13, ProbSets 9-12,& DAIT 7,8 12/17:  FINAL EXAM
2:30-4:30 p.m.
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Data and Statistics  |  Solubility, Acid/Base and Simultaneous Equilibria
Electrochemistry | SpectroscopyChromatography and Separations


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