Analytical
Chemistry
Chemistry 255/256
Fall 2003
Course Calendar
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Monday
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Tuesday
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Wednesday
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Thursday
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Friday
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Sep 1
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2
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3
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4 Class 1
Introduction to
role-playing laboratories and classes. Workshop: Preparing a Professional
Quality Graph
Harris
Ch 3
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5
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8
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9 Class
2
Standard
deviations, confidence intervals, and Statistical Tests.
Harris
Ch 4
• ProbSet
1 DUE
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10
Lab 2- Basic Skills
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11 Class
3
Statistical
and round robin testing of laboratory data using the Q-test, t-test and
F-test. Workshop: BP data
Harris
Ch 5, §28-1
• DAIT
1 DUE
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12
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15
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16 Class 4 Solubility 1-control of solution species and
composition with common ions
Harris
§9-1 thru 9-3, 6-1 thru 6-6
• ProbSet
2 DUE
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17
Lab 3- Glassware
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18 Class 5
Quiz 1 (20 min.)
Alpha
fractions as computational tools in equilibria problems.
Workshop: Alpha Fractions
Harris
§11-5
• DAIT
2 DUE
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19
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22
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23 Class
6
Solubility
2 - Computational tools and pH control of solution composition.
Harris
§9-4
• ProbSet
3 DUE
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24
Lab 4- Oxalate
1
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25 Class
7
Solubility
3 - Effect of ionic strength (activities) on solubility.
Workshop: Ionic Strength
effects
Harris Ch 8
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26
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29
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30 Class
8
Acid/Base
1 - How to do monoprotic weak acids and buffer solutions.
Harris
§6-7 thru 6-9, Ch 10
• ProbSet
4 DUE
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Oct 1
Lab 5- Oxalate
2
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2 Class
9
Acid/Base 2 - How to approach polyprotic buffer
equilibria problems.
Harris
Ch 11
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3
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6
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7 Class
10
Examination 1
Covering
Classes 1-7, Labs 1-5, ProbSets 1-4, & DAIT 1-2
• ProbSet
5 DUE
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8
Lab 6-Acid1
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9 Class
11
Literature
Searching and Reference Management. Acid/Base 3 - Amphoteric
buffer systems and pH problems.
Harris
§11-1
• DAIT
3 DUE
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10
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13
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14 Class
12
Acid/Base
4 - Polyprotic titrations and stoichiometry.
Harris
§12-1 thru 12-4
• ProbSet
6 DUE
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15
Lab 7-Acid2
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16 Class 13
Acid Base 5 - Titrations
as an analytical method.
Workshop: Endpoint
Determination
Harris
§12-5 thru 12-9
• DAIT
4 DUE
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17
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20
Fall Break
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21
Fall Break
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22
No Lab This Week
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23 Class
14
Spectrophotometry
1 - Interaction of light with matter
Workshop: Spectroscopy
in Nature
Harris
Ch 18
• DAIT 5 DUE
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24
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27
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28 Class
15
Quiz
2 (20 Min.)
Spectrophotometry
2 – Atomic Spectroscopy.
Video: Robotics in the Analytical Laboratory
Harris
Ch 21
• ProbSet
7 DUE
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29
Lab 8-Mock Robot
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30 Class
16
Spectrophotometry
3 – Spectrophotometers and UV/Vis systems.
Harris
Ch 20
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31
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Nov 3
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4 Class
17
Spectrophotometry 4 – Applications
of Spectroscopy
Workshop: Spectroscopy of
Mixtures
Harris
Ch 19
• ProbSet
8 DUE
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5
Lab 9-Easter Egg
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6 Class 18
Redox 1- Equilibrium
cell potentials via the IUPAC conventions & the Nernst equation
Harris
Ch 14
• DAIT 6 DUE
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7
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10
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11 Class
19
Redox
2 – Electrodes and Appllications of electrodes.
Harris Ch 15
• ProbSet 9 DUE
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12
Lab 10-Downsizing
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13 Class
20
Examination
2
Covering
Classes 11-19, Labs 6-9, ProbSets 5-9, & DAIT 3-6
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14
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17
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18 Class
21
Redox
3 - Applying the Nernst equation to potentiometric titrations.
Harris
Ch 16
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19
Lab 11-Pill Machine
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20 Class
22
Separations
1 – Solvent Extraction as a single stage chromatography experiment
Harris
Ch 23
• DAIT 7 DUE
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21
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24
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25 Class
23
Separations 2 - Theoretical plates,
peak shape and gas chromatography.
Harris
Ch 24
• ProbSet
10 DUE 6
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26
Thanksgiving Break
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27
Thanksgiving Break
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28
Thanksgiving Break
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Dec 2
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3 Class
24
Separations
3 – Pumps, columns and detectors in HPLC.
Harris
Ch 25
• ProbSet 11 DUE
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4
Lab 12 - HPLC
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5 Class
25
Quiz
3 (20 Min.)
Separations
4 – Capillary Electrophoresis and Chromatographic Applications.
Harris
Ch 26
• DAIT
8 DUE
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6
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8
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9 Class
26
LAST
DAY OF CLASS
Separations 5 –
Workshop: analysis of
chromatogram and the quality of separation
• ProbSet 12 DUE
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10
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11 Reading Day
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12
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15
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16
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17
FINAL
EXAM
2:30-4:30 p.m.
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18
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19
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