|
#
|
Day
|
Date
|
Lecture Topic
|
(c)Class Mat'l
|
Reading
|
Assigned
|
Due
|
| 1 | Fri | 9/6 | Introduction to Instrumental Analysis - Negotiations for Labs | Notes | 1-19, 21-24 |
Sim1
|
- |
| 2 | Mon | 9/9 | The Voltage-Divider Equation as a Calculational Tool | Templates | 24-28 |
PS1
|
- |
| 3 | Wed | 9/11 | The Superposition Principle and the Null-T Voltage Divider | Templates | 28-49 |
Sim2
|
Sim1
|
| 4 | Fri | 9/13 | Conceptual Introduction to Operational Amplifiers | Templates | 53-58 |
PS2
|
PS1
|
| 5 | Mon | 9/16 | Virtual Ground Concept and Voltage-Driven Op-Amps | Templates | 59-68 |
Sim3
|
Sim2
|
| 6 | Wed | 9/18 | Virtual Ground in Current and Voltage Follower Op-Amps | Templates | 99-113 |
PS3
|
PS2
|
| 7 | Fri | 9/20 | Derivation of the Ilkovic Equation (Part 1) | Notes | 639-648 |
Sim4
|
Sim3
|
| 8 | Mon | 9/23 | Derivation of the Ilkovic Equation (Part 2) | Notes | 648-654 |
Sim5
|
PS3
|
| 9 | Wed | 9/25 | Computer Operation of a Static Mercury Drop Electrode | Templates | 654-670 | - |
Sim4
|
| 10 | Fri | 9/27 | Demo of Computer-Controlled Electrochemical Methods | Lab Demo | 73-96 |
Sim6
|
Sim5
|
| (10) | Fri | 9/27 | Exam #1 - Handed Out | Exam | Covers all mat'l for Lectures 1-10, Labs 1-3, Sims 1-4, Problem Sets 1-3 |
||
| (11) | Mon | 9/30 | Exam #1 - Handed In | Answers | |||
|
11
|
Mon
|
9/30
|
Design of a Czerny-Turner Monochromator - PMT Detection
|
Templates
|
157-171
|
PS4
|
-
|
|
12
|
Wed
|
10/2
|
Design of a Generic, Double-Beam Spectrophotometer
|
Templates
|
312-325
|
Sim7
|
Sim6
|
|
13
|
Fri
|
10/4
|
How a Charge-Coupled Device (CCD) Works
|
Notes
|
172-176
|
PS5
|
PS4
|
|
14
|
Mon
|
10/7
|
Design of an Ebert Spectrograph with CCD Detection
|
Notes
|
73-89
|
Sim8
|
Sim7
|
|
15
|
Wed
|
10/9
|
Instrumental Bandpass Caused by Spectrometer Design
|
Templates
|
300-312
|
PS6
|
PS5
|
|
16
|
Fri
|
10/11
|
Using LabVIEW to Explore Effects of Bandpass
|
-
|
Simulation 8
|
Sim9
|
Sim8
|
|
17
|
Mon
|
10/14
|
Electrical Discharges as Emission Light Sources
|
Templates
|
230-251
|
PS7
|
PS6
|
|
18
|
Wed
|
10/16
|
The Uniquesness of the Atomic Absorption Experiment
|
Templates
|
192-204
|
Sim10
|
Sim9
|
|
19
|
Fri
|
10/18
|
Flame Cells for the Atomic Absorption Experiment
|
Templates
|
206-210
|
Sim11
|
PS7
|
|
-
|
Mon
|
10/21
|
No Class Due to Fall Break
|
-
|
|||
|---|---|---|---|---|---|---|---|
|
20
|
Wed
|
10/23
|
The Graphite Furnace as an Atomic Absorption Cell
|
Templates
|
210-214
|
PS8
|
Sim10
|
|
21
|
Fri
|
10/25
|
Using LabVIEW to Visualize a Double-Beam AA
|
-
|
215-227, Sim9
|
Sim12
|
PS8
|
|
(21)
|
Fri
|
10/25
|
Exam #2 - Handed Out
|
Exam
|
Covers all mat'l for Lectures 11-21,
Labs 4-6, Sims 5-10, Problem Sets 4-8 |
||
|
(22)
|
Mon
|
10/28
|
Exam #2 - Handed In
|
Answers
|
|||
| 22 | Mon | 10/28 | The Fourier Transform Approach to IR Spectrometry | Templates | 404-426 |
PS9
|
- |
| 23 | Wed | 10/30 | Optical Principles of the Michelson Interferometer | Templates | 182-189 |
Sim13
|
Sim11
|
| 24 | Fri | 11/1 | The Algebra of Fourier Transformation | Templates | 380-401 |
PS10
|
PS9
|
| 25 | Mon | 11/4 | Cross Correlation for Discrete Fourier Transformation | Templates | Simulation 12 |
Sim14
|
Sim12
|
| 26 | Wed | 11/6 | Using LabVIEW to Study Apodization and Resolution | - | Simulation 13 |
PS11
|
PS10
|
| 27 | Fri | 11/8 | Using LabVIEW for FT/IR Spectral Subtraction | - | Simulation 10 |
Sim15
|
Sim13
|
| 28 | Mon | 11/11 | FT/NMR 1 - The Basic NMR Pulsed Absorption Experiment | Templates | 445-450, 470-473 |
PS12
|
PS11
|
| 29 | Wed | 11/13 | FT/NMR 2 - Generating the Pulsed RF Absorption Signal | Templates | 470-459 |
Sim16
|
Sim14
|
| 30 | Fri | 11/15 | FT/NMR 3 - Analyzing the Free Induction Decay | Templates | 459-469 |
PS13
|
PS12
|
| 31 | Mon | 11/18 | FT/NMR 4 - Sidebanding for Carrier Demodulation | Templates | 450-457 |
Sim17
|
Sim15
|
| 32 | Wed | 11/20 | FT/NMR 5 - Coordinate Rotation for Detection Phasing | Notes | - |
PS14
|
PS13
|
| 33 | Fri | 11/22 | FT/NMR 6 - How MRI Works | Notes | 473-491 | - |
Sim16
|
| (33) | Fri | 11/22 | Exam #3 - Handed Out | Exam | Covers all mat'l for Lectures 22-33, Labs 7-9, Sims 11-17, Problem Sets 9-13 |
||
| (34) | Mon | 11/25 | Exam #3 - Handed In | Answers | |||
| - | Wed | 11/27 | No Class Due to Thanksgiving Break | - | |||
| - | Fri | 11/29 | |||||
| 34 | Mon | 11/25 | Types of Gas and Liquid Partition Chromatography Columns | Templates | 674-694 |
Sim18
|
- |
| 35 | Mon | 12/2 | Types of Pumps and Injectors for HPLC | Templates | 728-738 | - |
Sim17
|
| 36 | Wed | 12/4 | Types of Detectors for HPLC | Templates | 701-721 |
PS15
|
PS14
|
| 37 | Fri | 12/6 | Components for a Packed Column GC/MS Instrument | Templates | 739-765 |
Sim19
|
Sim18
|
| 38 | Mon | 12/9 | Impact Ionization and the Quad Mass Spectrometer | Templates | 498-518 | - |
PS15
|
| 39 | Wed | 12/11 | Chemical Ionization and the TOF Mass Spectrometer | Templates | 519-532 | - |
Sim19
|