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Chemistry 378 – Instrumental Analysis Lab for Fall, 2002 Experiment Schedule |
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Sun |
Monday |
Tuesday |
Wednesday |
Thursday |
Friday |
Sat |
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1 |
2 Week 1 Activities |
3 |
4 |
5 Classes Start LabVIEW Tutorials: 3 people at 1:30 and 3 at 3:30 in SC 321/328 |
6 Class 1 3 people at 1:30 and 3 at 3:30 in SC 321/328 |
7 |
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8 |
9 Class 2 SM to explain BCD number and digital port representations |
10 Lab 1 Week - DIOMaking a Digital pH Meter – Wiring BCD Connector - Hardware |
11 Class 3 Making a Digital pH Meter – Building the Front Panel - Software |
12 Using the Digital pH Meter – Plot Electrode Response - Chemist |
13 Class 4 Storyboard on Measuring Responses with Digital pH Meter |
14 |
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15 |
16 Class 5SM to explain A/D conversion by serial connection |
17 Lab 2 Week – A/D Building a RS-232 null modem to couple two serial terminals |
18 Class 6Using an RS-232 level shifter to operate a serial A/D converter |
19 Using an RS-232 level shifter to operate a serial DVM meter |
20 Class 7Storyboard on serial RS-232 A/D conversion methods. |
21 |
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22 |
23 Class 8.SM to explain OP-amp and instrumentation amp used with DVM’s |
24 Lab 2 Week – OA Building an instru- |
25 Class 9Building an active attenuator to unload & DVM read voltages |
26 Building a current follower to DVM read LED photo-signals . |
27 Class 10Storyboard on using operational amps for signal conditioning. |
28 |
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29 |
30 Class 11SM to explain A/D conversion icons in LabVIEW |
1 Oct Lab 3 Wk A/DMeasuring High Level signal – Function Generator - Software |
2Class 12Measuring High Level signals with active attenuator - Hardware |
3 Measuring Physio-logical signal with AD620 amp- Chemist |
4 Class 13Storyboard on A/D Conversion w/ AD620 Instr. Amp |
5 |
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6 |
7 Class 14SM to explain D/A conversion icons |
8 Lab 4 Wk – D/ADefining Special Chemical Waveforms - Chemist |
9 Class 15Plotting Special Chemical Waveforms - Software |
10 Recording Special Chemical Waveforms - Hardware |
11 Class 16 Storyboard on Computer-Generated Chemical Waveforms |
12 |
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13 |
14 Class 17SM to setup Mock GC Oven |
15 Lab 6 Week - ALLMock GC Oven – Tracing the Circuitry – Lamp & Fan Control |
16 Class 18Mock GC Oven – Measuring the Hot- Zone Temperature |
17 Mock GC Oven – Complete Hot-Zone Temperature Control |
18 Class 19Storyboard of Mock GC Oven Temp. LabVIEW Controllers |
19 |
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20 |
21 Fall Break Mike gets ready to give tutorials |
22 Fall Break Mike gets ready to give tutorials |
23 Class 20 Robot Tutorials: 3 people at 1:30 and 3 at 3:30 – room 328. |
24Robot Tutorials: 3 people at 1:30 and 3 at 3:30 – room 328. |
25 Class 21Storyboard on Mike the Zymark Lab Robot in Operation |
26 |
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27 |
28 Class 22 SM to setup AA for full lab roles – decide on water sample sites. |
29 Lab 7 WeekAtomic Absorption - Standard Addition Solution Design Full Company A |
30 Class 23 Atomic Absorption - Robot Standard Addition Preparation Full Company B |
31 Atomic Absorption – St.Olaf Water Robot Assisted Analysis Full Company C |
1 Nov Class 24 – Storyboard on Standard Addition AA Water Analysis with Robot Assistance |
2 |
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3 |
4 Class 25 SM to setup FT/IR for full lab roles – decide on spray sample types. |
5 Lab 8 WeekFT/IR Spectral Subtraction Project Full Company A |
6 Class 26FT/IR Spectral Subtraction Project – Full Company B |
7 FT/IR Spectral Subtraction Project – Full Company C |
8 Class 27 Storyboard on FT/IR Difference Spectra for product comparison |
9 |
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10 |
11 Class 28 SM on Building NMR VI to display spectra & sub-VI responsibilities |
12 Lab 9 Week LabVIEW NMR sub-VI for getting data into real and imag. FT |
13 Class 29 LabVIEW NMR sub-VI for quadrature array manipulation of NMR |
14 LabVIEW NMR sub-VI for doing phasing adjustments |
15 Class 30 Storyboard on NMR processing and spectral display VI |
16 |
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17 |
18 Class 31 SM to setup robot for whole class roles – plan lab responsibilities |
19 Lab 11a WeekRobot Aspirin Hydrolysis Setup – Full Company A |
20 Class 32 Robot Aspirin Hydrolysis Reagents – Full Company B |
21 Robot Aspirin Hydrolysis Program – Full Company C |
22 Class 33 Storyboard Showing of Robot Methods Development |
23 |
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24 |
25 Class 34 SM to prepare robot system for long data run over break |
26 Lab 11b Week Start Robot on Aspirin Hydrolysis Companies A, B, & C |
27 Thanksgiving BreakMike takes an aspirin |
28 Thanksgiving BreakMike takes an aspirin |
29 Thanksgiving BreakMike takes an aspirin |
30 |
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1 |
2 Class 35 SM on RP-HPLC mock gasoline spill workstation. |
3 Lab 12 Week RP-HPLC - Chemistry of Mock Gasoline Spill Problem |
4 Class 36 RP-HPLC –Software of Mock Gasoline Spill Problem |
5 RP-HPLC –Hardware of Mock Gasoline Spill Problem |
6 Class 37 Storyboard on Mock Gasoline Spill Problem & HPLC workstation |
7 |
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8 |
9 Class 38 |
10 No Lab |
11 Class 39 |
12 Reading Day |
13 Final exam week starts – ends 19 Dec |
14 |