Chemistry 378 Instrumental Analysis Lab for Fall, 2002 Experiment Schedule

Sun

Monday

Tuesday

Wednesday

Thursday

Friday

Sat

1

2 Week 1 Activities

3

4

5 Classes Start

LabVIEW Tutorials:

3 people at 1:30 and 3 at 3:30 in SC 321/328

6 Class 1
LabVIEW Tutorials:

 3 people at 1:30 and 3 at 3:30 in SC 321/328

7

8

9 Class 2

SM to explain BCD number and digital port representations

10 Lab 1 Week - DIO

Making a Digital pH Meter Wiring BCD Connector - Hardware

11 Class 3

Making a Digital pH Meter Building the Front Panel - Software

12

Using the Digital pH Meter Plot Electrode Response - Chemist

13 Class 4

Storyboard on Measuring Responses with Digital pH Meter

14

15

16 Class 5

SM to explain A/D conversion by serial connection

17 Lab 2 Week A/D Building a RS-232 null modem to couple two serial terminals

18 Class 6

Using an RS-232 level shifter to operate a serial A/D converter

19

Using an RS-232 level shifter to operate a serial DVM meter

20 Class 7

Storyboard on serial RS-232 A/D conversion methods.

21

22

23 Class 8

.SM to explain OP-amp and instrumentation amp used with DVMs

24 Lab 2 Week OA

Building an instru-
mentation amp for DVM thermocouples

25 Class 9

Building an active attenuator to unload & DVM read voltages

26

Building a current follower to DVM read LED photo-signals .

27 Class 10

Storyboard on using operational amps for signal conditioning.

28

29

30 Class 11

SM to explain A/D conversion icons in LabVIEW

1 Oct Lab 3 Wk A/D

Measuring High Level signal Function Generator - Software

2Class 12

Measuring High Level signals with active attenuator - Hardware

3

Measuring Physio-logical signal with AD620 amp- Chemist

4 Class 13

Storyboard on A/D Conversion w/ AD620 Instr. Amp

5

6

7 Class 14

SM to explain D/A conversion icons

8 Lab 4 Wk D/A

Defining Special Chemical Waveforms - Chemist

9 Class 15

Plotting Special Chemical Waveforms - Software

10

Recording Special Chemical Waveforms - Hardware

11 Class 16

Storyboard on Computer-Generated Chemical Waveforms

12

13

14 Class 17

SM to setup Mock GC Oven

15 Lab 6 Week - ALL

Mock GC Oven Tracing the Circuitry Lamp & Fan Control

16 Class 18

Mock GC Oven Measuring the Hot- Zone Temperature

17

Mock GC Oven Complete Hot-Zone Temperature Control

18 Class 19

Storyboard of Mock GC Oven Temp. LabVIEW Controllers

19

20

 

21

Fall Break

Mike gets ready to give tutorials

22

Fall Break

Mike gets ready to give tutorials

23 Class 20

Robot Tutorials:

3 people at 1:30 and 3 at 3:30 room 328.

24

Robot Tutorials:

3 people at 1:30 and 3 at 3:30 room 328.

25 Class 21

Storyboard on Mike the Zymark Lab Robot in Operation

26

27

28 Class 22

SM to setup AA for full lab roles decide on water sample sites.

29 Lab 7 Week

Atomic Absorption - Standard Addition Solution Design

Full Company A

30 Class 23

Atomic Absorption - Robot Standard Addition Preparation

Full Company B

31

Atomic Absorption St.Olaf Water Robot Assisted Analysis

Full Company C

1 Nov Class 24

Storyboard on Standard Addition AA Water Analysis with Robot Assistance

2

3

4 Class 25

SM to setup FT/IR for full lab roles decide on spray sample types.

5 Lab 8 Week

FT/IR Spectral Subtraction Project Full Company A

6 Class 26

FT/IR Spectral Subtraction Project

Full Company B

7

FT/IR Spectral Subtraction Project

Full Company C

8 Class 27

Storyboard on FT/IR Difference Spectra for product comparison

9

10

11 Class 28

SM on Building NMR VI to display spectra & sub-VI responsibilities

12 Lab 9 Week

LabVIEW NMR sub-VI for getting data into real and imag. FT

13 Class 29

LabVIEW NMR sub-VI for quadrature array manipulation of NMR

14

LabVIEW NMR sub-VI for doing phasing adjustments

15 Class 30

Storyboard on NMR processing and spectral display VI

16

17

18 Class 31

SM to setup robot for whole class roles plan lab responsibilities

19 Lab 11a Week

Robot Aspirin Hydrolysis Setup Full Company A

20 Class 32

Robot Aspirin Hydrolysis Reagents Full Company B

21

Robot Aspirin Hydrolysis Program Full Company C

22 Class 33

Storyboard Showing of Robot Methods Development

23

24

25 Class 34

SM to prepare robot system for long data run over break

26 Lab 11b Week

Start Robot on Aspirin Hydrolysis

Companies A, B, & C

27

Thanksgiving Break

Mike takes an aspirin

28

Thanksgiving Break

Mike takes an aspirin

29

Thanksgiving Break

Mike takes an aspirin

30

1

2 Class 35

SM on RP-HPLC mock gasoline spill workstation.

3 Lab 12 Week

RP-HPLC - Chemistry of Mock Gasoline Spill Problem

4 Class 36

RP-HPLC

Software of Mock Gasoline Spill Problem

5

RP-HPLC

Hardware of Mock Gasoline Spill Problem

6 Class 37

Storyboard on Mock Gasoline Spill Problem & HPLC workstation

7

8

9 Class 38

10 No Lab

11 Class 39

 

12 Reading Day

13 Final exam week

starts ends 19 Dec

14

 

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